pKa Tables - The mother of all pKa tables, 40+ pages (from CRC's Handbook of Biochemistry and Molecular Biology)
pKa's of Tertiary Amines - pKa's in both DMSO and water. Pretty handy. Table is about halfway down the paper
Grignard Titration - Paper and lab notebook page that show how to titrate Grignard reagents
Helpful Links for Synthetic Chemists
Not Voodoo - Tips and tricks for a number of common laboratory procedures (recrystallizations, etc)
Al's Notebook - Experimental protocols for a large number of basic transformations
ScienceCheck.org - New website that reviews published procedures
Physical Data Tables and Calculators
Organic Division Information - MASSIVE collection of data tables, includes almost everything you need to know, plus pages of syntheses, named reagents and reactions.
Bond Strength Tables - From the Lectka group, a massive collection of bond strengths